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Scientific Article   |    
New Polys for Old: Contribution or Caveat?
A. Seth Greenwald, DPhil(Oxon); Thomas W. Bauer, MD, PhD; Michael D. Ries, MD
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A. Seth Greenwald, DPhil(Oxon)
Orthopaedic Research Laboratories, Lutheran Hospital, Cleveland Clinic Health System, 1730 West 25th Street, Cleveland, OH 44113. E-mail address: seth@orl-inc.com

Thomas W. Bauer, MD, PhD
Department of Pathology, Cleveland Clinic Foundation, 9500 Euclid Avenue, L25, Cleveland, OH 44195

Michael D. Ries, MD
University of California San Francisco Medical Center, 500 Parnassus Avenue, MU 320-W, San Francisco, CA 94143

The authors did not receive grants or outside funding in support of their research or preparation of this manuscript. They did not receive payments or other benefits or a commitment or agreement to provide such benefits from a commercial entity. No commercial entity paid or directed, or agreed to pay or direct, any benefits to any research fund, foundation, educational institution, or other charitable or nonprofit organization with which the authors are affiliated or associated.

The Journal of Bone & Joint Surgery.  2001; 83:S27-31 
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The enduring success of the low-friction arthroplasty first advanced by Sir John Charnley as a solution for severe hip arthritic problems may be appreciated from the fact that in 1999 more than 500,000 hip and knee arthroplasties were performed in the United States. The prevalence of aseptic loosening attributed to polyethylene debris-induced osteolysis has been in the single digits in most contemporary series, with some reports describing prostheses surviving for twenty to thirty years (Figs. 1-A and 1-B).
Until recently, gamma irradiation in air has been the predominant method of sterilization of ultra-high molecular weight polyethylene components and, despite current concerns, it represents the only gold standard against which contemporary material improvements will be measured over time.
The ultra-high molecular weight polyethylene used in hip and knee arthroplasty components results from polymerization of ethylene gas into a fine resin powder of submicrometer and micrometer size distribution. It is consolidated with use of ram-extrusion or compression-molding techniques. Structurally, the polymer is made up of repeating carbon-hydrogen (-CH2-) units that are arranged in ordered (crystalline) and disordered (amorphous) regions. Irradiation to sterilize components breaks the polymer chains, creating free radicals, which in an air environment combine with oxygen, facilitating ongoing oxidative degradation of the polymer (Fig. 2).
Continued exposure of the component to oxygen through prolonged shelf storage in air before clinical use results in a progressive stiffening and embrittlement of the polymer, reducing wear resistance and fatigue strength. This is thought to represent a major contributing factor influencing in vivo polymer failure (Figs. 3 and 4).
Besides reacting with oxygen, however, free radicals can also combine, creating cross-links between adjacent molecules. Bench-testing has suggested that these cross-links improve wear performance. Eliminating oxygen from the sterilization process by employing inert gas or a vacuum environment contributes to this improvement.
Alternative sterilization methods employing ethylene oxide or gas plasma without ionizing radiation avoid oxidation but do not realize potential wear performance benefits resulting from increased cross-linking (Fig. 5).
Previous attempts to improve the performance of ultra-high molecular weight polyethylene have included carbon-fiber reinforcement (Poly-2) and, more recently, polymer reprocessing to enhance mechanical properties by hot isostatic pressing (Hylamer). The former was withdrawn from the market because of an unexpectedly high wear rate (Fig. 6), while the latter has been linked to debris-induced osteolytic response, especially when sterilized by radiation in air, in early reports (Fig. 7).
Heat pressing was yet another attempt to improve the finish of the articular surface, but it was associated with polyethylene fatigue and early delamination (Fig. 8).
These findings suggest that the preclinical evaluations of the above polyethylenes did not fully predict in vivo performance.
The new generation of cross-linked polyethylenes represents a class of emerging ultra-high molecular weight polyethylene alternatives whose common denominator is an appreciation of the importance of increased cross-linking and minimization of oxidative degradation to reduce wear. Both chemical and thermal/radiation processing solutions have been advocated, with a number of the latter being recently cleared by the Food and Drug Administration for commercial product distribution.
Process differences include: (1) heating above or below the melt temperature of the polyethylene, (2) the radiation source, (3) dose level, and (4) end-point sterilization (Fig. 9).
In general, increasing the radiation dose dramatically reduces polymer wear in laboratory hip joint simulation (Fig. 10). Free-radical suppression through kinetic recombination at increased temperature in an oxygen-free environment or quenching through remelting represent efforts to stem the oxidation process.
The above processes also change either the amorphous or both the amorphous and the crystalline regions of the resulting polymers, affecting mechanical properties and potentially reducing fatigue characteristics. Fatigue damage is a factor associated with high cyclic stresses in nonconforming ultra-high molecular weight polyethylene knee components. It is not known how these polyethylenes will perform in knees. Current market application is primarily limited to acetabular components, with limited Food and Drug Administration clearance for use in the knee.
There is some laboratory evidence suggesting that increased cross-linking may decrease resistance to fatigue crack propagation (Figs. 11-A and 11-B), a finding that could have implications for some modular acetabular cup designs (Fig. 12).
Currently, there is no direct clinical evidence of the promised long-term in vivo integrity, suggested by laboratory evaluation, of the cross-linked polymer being marketed today.
The absence of information on the long-term clinical performance of highly cross-linked ultra-high molecular weight polyethylene components prompted the Medical Devices Agency of the United Kingdom in June 1999 to issue a Safety Notice (MDA SN1999[23]) advising caution in their use and careful patient monitoring.
For the past three decades, ultra-high molecular weight polyethylene hip and knee components have been predominantly sterilized by gamma irradiation in air and have shown remarkable overall resilience in terms of clinical function.
Nevertheless, aseptic loosening attributed to polyethylene debris-induced osteolysis is of contemporary concern. As the indications for total joint replacement expand to younger patients and life expectancy increases, the interest in alternative bearing materials has accelerated.
It is now known that irradiation in an environment in which oxygen is present encourages oxidation of ultra-high molecular weight polyethylene components, resulting in embrittlement and a decrease in wear performance. This process continues when components are shelf-stored in air or in permeable packaging for prolonged periods before use.
Sterilization in oxygen-free environments with barrier packaging and shelf-dating reduce the risk of material compromise.
The use of ethylene oxide and gas plasma as alternative sterilization methods avoids oxidative degradation, but there is loss of the potential benefits with respect to polymer wear reduction derived from cross-linking.
Recently a number of "improved" polymers have emerged whose common benefit resides in increased cross-linking concurrent with minimization of oxidation. Pin-on-disk testing has not been shown to predict in vivo performance, but hip simulator models suggest a significant reduction in wear with these new polymers.
These processes, however, change the chemical structure of the polymer, affecting both static mechanical properties and fatigue characteristics.
A number of these polyethylenes have received clearance by the Food and Drug Administration and are commercially available despite the absence of clinical reports.
Corporate responsibility to assess short-term performance by means of evidence-based studies is necessary and should be a consideration in the surgeon’s selection of highly cross-linked polymer components.
 
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+Fig. 1-A:Radiographs of a Charnley cemented hip replacement, made immediately postoperatively (Fig. 1-A) and twenty-five years postoperatively (Fig. 1-B).
 
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+Fig. 1-B:Radiographs of a Charnley cemented hip replacement, made immediately postoperatively (Fig. 1-A) and twenty-five years postoperatively (Fig. 1-B).
 
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+Fig. 2:Depiction of polymer chain breakage following irradiation in air and combination with oxygen, facilitating oxidative degradation of ultra-high molecular weight polyethylene.
 
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+Fig. 3:The influence of shelf storage on survival of a prosthetic knee plateau following gamma irradiation in air (Reproduced, with modification, from: Bohl JR, Bohl WR, Postak PD, Greenwald AS. The effects of shelf life on clinical outcome for gamma sterilized polyethylene tibial components. Clin Orthop. 1999;367:32. Reprinted with permission.)
 
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+Fig. 4:A Group-2 plateau (see Fig. 3) implanted after 7.6 years of shelf storage and retrieved 3.8 years after implantation. Gross delamination and pitting, characteristic of fatigue failure, are observed.
 
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+Fig. 5:Hip-simulator weight-loss comparison for aged (twenty-five days at 78°C in oxygen) compression-molded cup components. a = irradiated in air, b = sterilized with ethylene oxide, and c = irradiated in a vacuum environment and use of barrier packaging. (Reproduced, with modification, from: Greer KW, Schmidt MB, Hamilton JV. The hip simulator wear of gamma-vacuum, gamma-air, and ethylene oxide sterilized UHMWPE following a severe oxidative challenge. Trans Orthop Res Soc. 1998;23:52. Reprinted with permission.)
 
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+Fig. 6:Fig. 6 A failed Poly-2 tibial insert retrieved five years after implantation.
 
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+Fig. 7:Fig. 7 A failed Hylamer acetabular cup insert retrieved three years after implantation.
 
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+Fig. 8:Fig. 8 A heat-pressed tibial component retrieved six years after implantation.
 
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+Fig. 9:Current methods used to manufacture moderately to highly cross-linked polyethylene.
 
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+Fig. 10:Mean acetabular cup wear rates versus gamma dose level. (Reprinted, with permission, from: McKellop H, Shen F-W, Lu B, Campbell P, Salovey R. Development of an extremely wear-resistant ultra high molecular weight polyethylene for total hip replacements. J Orthop Res. 1999;17:160.)
 
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+Fig. 11-A:Figs. 11-A and 11-B Scanning electron micrographs of polyethylene fatigue fracture specimens. (Reprinted, with permission, from: Baker DA, Hastings RS, Pruitt L. Study of fatigue resistance of chemical and radiation crosslinked medical grade ultrahigh molecular weight polyethylene. J Biomed Mater Res. 1999;46:573-81.) Fig. 11-A Gas-plasma-sterilized specimen demonstrating ductile tearing associated with plastic deformation and slowing fatigue crack growth.
 
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+Fig. 11-B:Figs. 11-A and 11-B Scanning electron micrographs of polyethylene fatigue fracture specimens. (Reprinted, with permission, from: Baker DA, Hastings RS, Pruitt L. Study of fatigue resistance of chemical and radiation crosslinked medical grade ultrahigh molecular weight polyethylene. J Biomed Mater Res. 1999;46:573-81.) Fig. 11-B Radiation cross-linked specimen demonstrating the relative absence of ductile tearing mechanisms.
 
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+Fig. 12:Crack propagation failure of a retrieved acetabular cup associated with an inadequate locking-mechanism design.

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Anchor for JumpAnchor for Jump
+Fig. 1-A:Radiographs of a Charnley cemented hip replacement, made immediately postoperatively (Fig. 1-A) and twenty-five years postoperatively (Fig. 1-B).
Anchor for JumpAnchor for Jump
+Fig. 1-B:Radiographs of a Charnley cemented hip replacement, made immediately postoperatively (Fig. 1-A) and twenty-five years postoperatively (Fig. 1-B).
Anchor for JumpAnchor for Jump
+Fig. 2:Depiction of polymer chain breakage following irradiation in air and combination with oxygen, facilitating oxidative degradation of ultra-high molecular weight polyethylene.
Anchor for JumpAnchor for Jump
+Fig. 3:The influence of shelf storage on survival of a prosthetic knee plateau following gamma irradiation in air (Reproduced, with modification, from: Bohl JR, Bohl WR, Postak PD, Greenwald AS. The effects of shelf life on clinical outcome for gamma sterilized polyethylene tibial components. Clin Orthop. 1999;367:32. Reprinted with permission.)
Anchor for JumpAnchor for Jump
+Fig. 4:A Group-2 plateau (see Fig. 3) implanted after 7.6 years of shelf storage and retrieved 3.8 years after implantation. Gross delamination and pitting, characteristic of fatigue failure, are observed.
Anchor for JumpAnchor for Jump
+Fig. 5:Hip-simulator weight-loss comparison for aged (twenty-five days at 78°C in oxygen) compression-molded cup components. a = irradiated in air, b = sterilized with ethylene oxide, and c = irradiated in a vacuum environment and use of barrier packaging. (Reproduced, with modification, from: Greer KW, Schmidt MB, Hamilton JV. The hip simulator wear of gamma-vacuum, gamma-air, and ethylene oxide sterilized UHMWPE following a severe oxidative challenge. Trans Orthop Res Soc. 1998;23:52. Reprinted with permission.)
Anchor for JumpAnchor for Jump
+Fig. 6:Fig. 6 A failed Poly-2 tibial insert retrieved five years after implantation.
Anchor for JumpAnchor for Jump
+Fig. 7:Fig. 7 A failed Hylamer acetabular cup insert retrieved three years after implantation.
Anchor for JumpAnchor for Jump
+Fig. 8:Fig. 8 A heat-pressed tibial component retrieved six years after implantation.
Anchor for JumpAnchor for Jump
+Fig. 9:Current methods used to manufacture moderately to highly cross-linked polyethylene.
Anchor for JumpAnchor for Jump
+Fig. 10:Mean acetabular cup wear rates versus gamma dose level. (Reprinted, with permission, from: McKellop H, Shen F-W, Lu B, Campbell P, Salovey R. Development of an extremely wear-resistant ultra high molecular weight polyethylene for total hip replacements. J Orthop Res. 1999;17:160.)
Anchor for JumpAnchor for Jump
+Fig. 11-A:Figs. 11-A and 11-B Scanning electron micrographs of polyethylene fatigue fracture specimens. (Reprinted, with permission, from: Baker DA, Hastings RS, Pruitt L. Study of fatigue resistance of chemical and radiation crosslinked medical grade ultrahigh molecular weight polyethylene. J Biomed Mater Res. 1999;46:573-81.) Fig. 11-A Gas-plasma-sterilized specimen demonstrating ductile tearing associated with plastic deformation and slowing fatigue crack growth.
Anchor for JumpAnchor for Jump
+Fig. 11-B:Figs. 11-A and 11-B Scanning electron micrographs of polyethylene fatigue fracture specimens. (Reprinted, with permission, from: Baker DA, Hastings RS, Pruitt L. Study of fatigue resistance of chemical and radiation crosslinked medical grade ultrahigh molecular weight polyethylene. J Biomed Mater Res. 1999;46:573-81.) Fig. 11-B Radiation cross-linked specimen demonstrating the relative absence of ductile tearing mechanisms.
Anchor for JumpAnchor for Jump
+Fig. 12:Crack propagation failure of a retrieved acetabular cup associated with an inadequate locking-mechanism design.
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These activities have been planned and implemented in accordance with the Essential Areas and policies of the Accreditation Council for Continuing Medical Education (ACCME) through the joint sponsorship of the American Academy of Orthopaedic Surgeons and The Journal of Bone and Joint Surgery, Inc. The American Academy of Orthopaedic Surgeons is accredited by the ACCME to provide continuing medical education for physicians.
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